We investigated oxidation time dependence of graphene oxide employing modified Hummer method by dynamic light scattering. Oxidation reaction proceeded rapidly within about 24 hours, and was saturated. It is suggested that graphene oxides were not able to freely fragment. This implies that the oxidation reactions occur at the limited sites.

The numerical dispersibility measurement system was fabricated based on optical transparency to objectively evaluate undetectable dispersibility by naked eyes. The small deference of dispersibility and the dispersibility behaviors were simultaneously elucidated by the system. The abundance of octadecyl groups was also discussed from the result of dispersibility behaviors. The objective numerical evaluation is needed for precise analysis of dispersibility with respect to graphene, graphene derivatives and graphene related materials.